Gas Thermometry

mercury, manometer, temperature, volume, bulb, space, pressure, constant and scale

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In addition to the above, there are mixed methods in which both p and V or M are variable, such as those employed by Rud berg or Becquerel; but these are unsatisfactory for precision, as not leading to a sufficiently definite thermometric scale. There is also a variation' of the constant-volume method (ii.), in which the pressure is measured by the volumetric compression of an equal mass of gas kept at a constant temperature, instead of by a manometer.

Construction of Apparatus.—The manometric or constant volume method was selected by Regnault as the standard, and has been most generally adopted since his time. His apparatus has not been modified except in points of detail. A description of his instrument will be found in most text-books on heat.

A simple and convenient form of the instrument for general use is Jolly's (described in Poggendorff's Jubelband, p. 82, 1874), and represented in fig. 3. The two vertical tubes of the manometer are connected by an india-rubber tube properly strengthened by a cotton covering, and they can be made to slide vertically up and down a wooden pillar which supports them ; they are provided with clamps for fixing them in any position and a tangent screw for fine adjustment. The connection between the bulb and the manometer is made by means of a three-way tap. The scale of the instrument is engraved on the back of a strip of plane mirror before silvering, and the divisions are carried sufficiently far across the scale for the reflections of the two surfaces of the mercury to be visible behind the scale. Par allax can thus be avoided and an accurate reading obtained without the necessity of using a cathetometer. In order to allow for the expansion of the glass of the reservoir a weight-ther mometer bulb is supplied with the instrument, made from an other specimen of the same kind of glass, and the relative expan sion of the mercury and the glass can thus be determined by the observer himself. The volume of the air-bulb and that of the capillary tube and the small por tion of the manometer tube above the small beak of glass, the point of which serves as the fidu cial mark, are determined by the instrument-makers. The improve ments introduced by Chappuis, of the International Bureau at Sevres, in the construction of the con stant-volume hydrogen thermometer selected by the committee for the determination of the normal scale, are described in the text-books (e.g., Watson's Physics).

Pressure Correction.

In the practical application of the manometric method there are certain corrections peculiar to the method, of which account must be taken in work of precision.

The volume of the bulb is not accurately constant, but varies with change of pressure and temperature. The thermal expan sion of the bulb is common to all methods, and will be considered in detail later. The pressure correction is small, and is determined in the same manner as for a mercury thermometer. The value so

determined, however, does not apply strictly except at the tem perature to which it refers. If the pressure-coefficient were con stant at all temperatures and equal to e, the pressure correction, dt, at any point t of the scale would be obtainable from the simple formula where po is the initial pressure at the temperature T2. But as the coefficient probably varies in an unknown manner, the correc tion is somewhat uncertain, especially at high temperatures. An other very necessary but somewhat troublesome correction is the reduction of the manometer readings to allow for the varying temperatures of the mercury and scale. Since it is generally impracticable to immerse the manometer in a liquid bath to secure certainty and uniformity of temperature, the temperature must be estimated from the readings of mercury thermometers sus pended in mercury tubes or in the air near the manometer. It is therefore necessary to work in a room specially designed to secure great constancy of temperature, and to screen the man ometer with the utmost care from the source of heat in measure ments of high temperature.

Stem-exposure.

In all gas thermometers it is necessary in practice that the part of the gas in contact with the mercury or other liquid in the manometer should not be heated, but kept at a nearly constant temperature. The space above the mercury, together with the exposed portion of the capillary tube connecting the manometer with the thermometric bulb, may be called the "dead space." If the volume of the dead space is kept as nearly as possible constant by adjusting the mercury always up to a fixed mark, the quantity of air in this space varies nearly in direct proportion to the pressure, i.e., in proportion to the temperature of the thermometric bulb at constant volume. This necessitates the application of a stem-exposure correction, the value of which is approximately given by the formula dt=rt(t—loo) /T2 (7) where r is the ratio of the volume of the dead space to the volume of the thermometric bulb, and is the mean tempera ture of the dead space, which is supposed to be constant. The magnitude of the correction is proportional to the ratio r, and increases very rapidly at high temperatures. If the dead space is 1 per cent of the bulb, the correction will amount to only one-tenth of a degree at 5o° C, but reaches 5° at C, and 3o° at i,000° C. It is for this reason important in high-tempera ture work to keep the dead space as small as possible and to know its volume accurately. With a mercury manometer, the volume is liable to a slight uncertainty on account of changes of shape in the rrimiscus, as it is necessary to use a wide tube in order to secure accurate measurements of pressure.

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